Hach NA5600 sc Na+ インストールガイド

DOC023.97.80590

NA5600 sc Na

+

04/2019, Edition 2

Installation

Instalación

Instalação

設置

설치

การติดตั้ง

English..............................................................................................................................3

Français......................................................................................................................... 38

Español.......................................................................................................................... 76

Português.................................................................................................................... 114

日本語........................................................................................................................... 152

한글............................................................................................................................... 187

ไทย.................................................................................................................................. 222

2

Table of contents

Specifications on page 3

Safety information on page 6

Product overview on page 7

Items to collect on page 10

Installation guidelines on page 10

Mechanical installation on page 11

Electrode installation on page 12

Electrical installation on page 15

Plumbing on page 26

Install the analyzer bottles on page 32

Specifications

Specifications are subject to change without notice.

Table 1 General specifications

Specification Details

Dimensions (W x H x D) Analyzer with enclosure: 45.2 x 68.1 x 33.5 cm (17.8 x 26.8 x 13.2 in.)

Analyzer without enclosure: 45.2 x 68.1 x 25.4 cm (17.8 x 26.8 x 10.0 in.)

Enclosure Analyzer with enclosure: NEMA 4/IP65

Analyzer without enclosure: IP65, PCBA housing

Materials: Polyol case, PC door, PC hinges and latches, 304/316 SST hardware

Weight Analyzer with enclosure: 20 kg (44.1 lb) with empty bottles, 21.55 kg (47.51 lb) with

full bottles

Analyzer without enclosure: 14 kg (30.9 lb) with empty bottles, 15.55 kg (34.28 lb)

with full bottles

Mounting Analyzer with enclosure: wall, panel or table

Analyzer without enclosure: panel

Protection class 1

Pollution degree 2

Installation category II

Power requirements 100 to 240 VAC, 50/60 Hz, ± 10%; 0.5 A nominal, 1.0 A maximum; 80 VA maximum

Operating temperature 5 to 50 °C (41 to 122 °F)

Operating humidity 10% to 80% relative humidity, non-condensing

Storage temperature -20 to 60 °C (-4 to 140 °F)

Number of sample streams 1, 2 or 4 with programmable sequence

Analog outputs Six isolated; 0–20 mA or 4–20 mA; load impedance: 600 Ω maximum

Connection: 0.644 to 1.29 mm

2

(24 to 16 AWG) wire; 0.644 to 0.812 mm

2

(24 to

20 AWG) recommended, twisted pair shielded wire

English 3

Table 1 General specifications (continued)

Specification Details

Relays Six; type: not powered SPDT relays, each rated at 5 A resistive, 240 VAC maximum

Connection: 1.0 to 1.29 mm

2

(18 to 16 AWG) wire; 1.0 mm

2

(18 AWG) stranded

recommended, 5–8 mm OD cable. Make sure that the field wiring insulation is rated

80 °C (176 °F) minimum.

Digital inputs Six, non-programmable, isolated TTL type digital input or as a relay/open-collector

type input

0.644 to 1.29 mm

2

(24 to 16 AWG) wire; 0.644 to 0.812 mm

2

(24 to 20 AWG)

stranded recommended

Fuses Input power: T 1.6 A, 250 VAC

Relays: T 5.0 A, 250 VAC

Fittings Sample line and sample bypass drain: 6-mm OD push-to-connect fitting for plastic

tubing

Chemical and case drains: 7/16-in. ID slip-on fitting for soft plastic tubing

Certifications

CE-compliant, CB, cETLus, TR CU-compliant, RCM, KC

Table 2 Sample requirements

Specification Details

Sample pressure 0.2 to 6 bar (3 to 87 psi)

Sample flow rate 100 to 150 mL/minute (6 to 9 L/hour)

Sample temperature 5 to 45 °C (41 to 113 °F)

Sample pH Analyzers without cationic pump: 6 to 10 pH

Analyzers with cationic pump: 2 to 10 pH

Sample acidity (equivalent CaCO

3

) Analyzers without cationic pump: Less than 50 ppm

Analyzers with cationic pump: Less than 250 ppm

Suspended solids in sample Less than 2 NTU, no oil, no grease

Table 3 Measurement specifications

Specification Details

Electrode type Sodium ISE (ion specific electrode) electrode and reference electrode with KCl

electrolyte

Measurement range Analyzers without cationic pump: 0.01 to 10,000 ppb

Analyzers with cationic pump: 0.01 ppb to 200 ppm

Accuracy Analyzers without cationic pump:

• 0.01 ppb to 2 ppb: ± 0.1 ppb

• 2 ppb to 10,000 ppb: ± 5%

Analyzers with cationic pump:

• 0.01 ppb to 40 ppb: ± 2 ppb

• 40 ppb to 200 ppm: ± 5%

Precision/Repeatability Less than 0.02 ppb or 1.5% (the larger value) with ± 10 °C (50 °F) sample

difference

4 English

Table 3 Measurement specifications (continued)

Specification Details

Interference phosphate 10 ppm Measurement interference is less than 0.1 ppb

Response time Refer to Table 4.

Stabilization time Startup: 2 hours; Sample temperature variation: 10 minutes from 15 to 30 °C

(59 to 86 °F)

Use the optional heat exchanger when the temperature difference between

samples is more than 15 °C (27 °F).

Calibration time 50 minutes (typical)

Calibration Automatic calibration: known addition method; Manual calibration: 1 or 2 points

Minimum detection limit 0.01 ppb

Auto calibration solution Approximately 500 mL of 10-ppm Sodium Chloride is used in 3 months with a 7-

day calibration interval.

Container: 0.5 L, HDPE with polypropylene caps

Reactivation solution Approximately 500 mL of 0.5M Sodium Nitrate is used in 3 months with a 24-

hour reactivation interval.

Container: 0.5 L, HDPE with polypropylene caps

3M KCl electrolyte Approximately 200 mL of 3M KCl electrolyte is used in 3 months.

Container: 200 mL, polycarbon

Conditioning solution Analyzers without cationic pump: Approximately 1 L of Diisopropylamine (DIPA)

is used in 2 months at 25 °C (77 °F) for a sample pH target of 11.2.

Approximately 1 L of DIPA is used in approximately 13 weeks at 25 °C (77 °F)

for a sample pH target of 10 to 10.5.

Analyzers with cationic pump: The usage rate of DIPA is dependent on the

selected Tgas/Twater ratio. With a ratio of 100% (i.e., the volume of sample is

equal to the volume of gas) the consumption of DIPA is approximately

90 mL/day.

Container: 1 L, glass with cap, 96 x 96.5 x 223.50 mm (3.78 x 3.80 x 8.80 in.)

Table 4 Average response times

T90% ≤ 10 minutes

Concentration change from one channel

to another

Maximum temperature

difference (°C)

Time to accuracy 0.1 ppb or 5%

Up (minutes) Down (minutes)

0.1 ↔ 5 ppb 3 9 27

0.1 ↔ 50 ppb 3 11 41

0.1 ↔ 200 ppb 3 9 45

< 0.1 ↔ 1 ppb

1

3 29 36

0.1 ↔ 50 ppb 15 11 41

General information

In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential

damages resulting from any defect or omission in this manual. The manufacturer reserves the right to

make changes in this manual and the products it describes at any time, without notice or obligation.

Revised editions are found on the manufacturer’s website.

1

Experiment was done with ultra pure water (estimated at 50 ppt) and 1 ppb standard.

English 5

Safety information

N O T I C E

The manufacturer is not responsible for any damages due to misapplication or misuse of this product including,

without limitation, direct, incidental and consequential damages, and disclaims such damages to the full extent

permitted under applicable law. The user is solely responsible to identify critical application risks and install

appropriate mechanisms to protect processes during a possible equipment malfunction.

Please read this entire manual before unpacking, setting up or operating this equipment. Pay

attention to all danger and caution statements. Failure to do so could result in serious injury to the

operator or damage to the equipment.

Make sure that the protection provided by this equipment is not impaired. Do not use or install this

equipment in any manner other than that specified in this manual.

Use of hazard information

D A N G E R

Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.

W A R N I N G

Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious

injury.

C A U T I O N

Indicates a potentially hazardous situation that may result in minor or moderate injury.

N O T I C E

Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special

emphasis.

Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument

could occur if not observed. A symbol on the instrument is referenced in the manual with a

precautionary statement.

Electrical equipment marked with this symbol may not be disposed of in European domestic or public

disposal systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to

the user.

This is the safety alert symbol. Obey all safety messages that follow this symbol to avoid potential

injury. If on the instrument, refer to the instruction manual for operation or safety information.

This symbol indicates that a risk of electrical shock and/or electrocution exists.

This symbol indicates the need for protective eye wear.

6 English

This symbol indicates that the marked item can be hot and should not be touched without care.

This symbol indicates that the marked item requires a protective earth connection. If the instrument is

not supplied with a ground plug on a cord, make the protective earth connection to the protective

conductor terminal.

Certification

C A U T I O N

This equipment is not intended for use in residential environments and may not provide adequate protection to

radio reception in such environments.

Canadian Radio Interference-Causing Equipment Regulation, IECS-003, Class A:

Supporting test records reside with the manufacturer.

This Class A digital apparatus meets all requirements of the Canadian Interference-Causing

Equipment Regulations.

Cet appareil numérique de classe A répond à toutes les exigences de la réglementation canadienne

sur les équipements provoquant des interférences.

FCC Part 15, Class "A" Limits

Supporting test records reside with the manufacturer. The device complies with Part 15 of the FCC

Rules. Operation is subject to the following conditions:

1. The equipment may not cause harmful interference.

2. The equipment must accept any interference received, including interference that may cause

undesired operation.

Changes or modifications to this equipment not expressly approved by the party responsible for

compliance could void the user's authority to operate the equipment. This equipment has been tested

and found to comply with the limits for a Class A digital device, pursuant to Part 15 of the FCC rules.

These limits are designed to provide reasonable protection against harmful interference when the

equipment is operated in a commercial environment. This equipment generates, uses and can

radiate radio frequency energy and, if not installed and used in accordance with the instruction

manual, may cause harmful interference to radio communications. Operation of this equipment in a

residential area is likely to cause harmful interference, in which case the user will be required to

correct the interference at their expense. The following techniques can be used to reduce

interference problems:

1. Disconnect the equipment from its power source to verify that it is or is not the source of the

interference.

2. If the equipment is connected to the same outlet as the device experiencing interference, connect

the equipment to a different outlet.

3. Move the equipment away from the device receiving the interference.

4. Reposition the receiving antenna for the device receiving the interference.

5. Try combinations of the above.

Product overview

D A N G E R

Chemical or biological hazards. If this instrument is used to monitor a treatment process and/or

chemical feed system for which there are regulatory limits and monitoring requirements related to

public health, public safety, food or beverage manufacture or processing, it is the responsibility of the

user of this instrument to know and abide by any applicable regulation and to have sufficient and

appropriate mechanisms in place for compliance with applicable regulations in the event of malfunction

of the instrument.

English 7

The sodium analyzer continuously measures very low concentrations of sodium in ultra-pure water.

Refer to Figure 1 and Figure 2 for an overview of the analyzer components.

The sodium analyzer is available with or without an enclosure. The analyzer with an enclosure is for

wall, panel or table mounting. The analyzer without an enclosure is for panel mounting. Refer to

Figure 1.

The sodium analyzer uses a sodium ISE (ion specific electrode) electrode and a reference electrode

to measure the sodium concentration of the water sample. The difference in potential between the

sodium and reference electrode is directly in proportion to the logarithm of sodium concentration as

shown by Nernst law. The analyzer increases the pH of the sample to a constant pH between

10.7 and 11.6 with a conditioning solution before the measurement to prevent interference from

temperature or other ions on the sodium measurement.

The door can be easily removed for better access during installation and maintenance procedures.

The door must be installed and closed during operation. Refer to Figure 3.

Figure 1 Product overview—external view

1 Overflow vessel 7 Analytics panel

2 Status indicator light (refer to Table 5 on page 10) 8 Calibration standard bottle

2

3 Display and keypad 9 Reactivation solution bottle

4 SD card slot 10 Sodium electrode

5 Analyzer without enclosure (panel mount) 11 Reference electrode

6 Analyzer with enclosure (wall, panel or table mount)

2

Only supplied with analyzers with the auto calibration option.

8 English

Figure 2 Product overview—internal view

1 Latch to open analytics panel 4 KCl electrolyte reservoir

2 Analytics panel (open) 5 Conditioning solution bottle

3 Power switch 6 Optional cationic pump

3

Figure 3 Door removal

3

The optional cationic pump is necessary for accurate measurements if the sample(s) plumbed to

the analyzer is less than pH 6.

English 9

Status indicator light

The status indicator light shows the status of the analyzer. Refer to Table 5. The status indicator light

is above the display.

Table 5 Status indicator description

Color Status

Green The analyzer is in operation with no warnings, errors or reminders.

Yellow The analyzer is in operation with active warnings or reminders.

Red The analyzer is not in operation due to an error condition. A serious problem has occurred.

Items to collect

Collect the items that follow to install the instrument. The items that follow are supplied by the user.

In addition, collect all of the personal protective equipment appropriate to the chemicals that are

handled. Refer to the current safety data sheets (MSDS/SDS) for safety protocols.

Fasteners to

mount the

analyzer on a

wall if

applicable (4x)

4

Level

Tape

measure

Drill Wire strippers Wire cutters

Deionized water

(or sample

water)

0.5M Sodium Nitrate,

500 mL

10-mg/L

Sodium

Chloride

Standard,

500 mL

3M KCl

electrolyte,

150 mL

Diisopropylamine,

99%, 1 L (or

Ammonia 28%, 1 L)

100 µm filter

for each

sample line

(optional)

Installation

C A U T I O N

Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the

document.

Installation guidelines

Install the analyzer:

• Indoors in a clean, dry, well-ventilated and temperature-controlled location.

• In a location with minimum mechanical vibrations and electronic noise.

• As close to the sample source as possible to decrease analysis delay.

• Near an open chemical drain.

• Away from direct sunlight and heat sources.

• So that the power cable plug is visible and easily accessible.

4

Use fasteners applicable to the mounting surface (¼-in. or 6 mm SAE J429-Grade 1 bolts or

stronger).

10 English

• In a location with sufficient space in front of it to open the door.

• In a location where there is sufficient clearance around it to make plumbing and electrical

connections.

This instrument is rated for an altitude of 2000 m (6562 ft) maximum. Use of this instrument at an

altitude higher than 2000 m can slightly increase the potential for the electrical insulation to break

down, which can result in an electric shock hazard. The manufacturer recommends that users with

concerns contact technical support.

Mechanical installation

D A N G E R

Risk of injury or death. Make sure that the wall mounting is able to hold 4 times the weight of the

equipment.

W A R N I N G

Personal injury hazard.

Instruments or components are heavy. Use assistance to install or move.

The object is heavy. Make sure that the instrument is securely attached to a wall, table or floor for a

safe operation.

Mount the analyzer indoors, in a non-hazardous environment.

Refer to the supplied mounting documentation.

English 11

Electrode installation

Install the reference electrode

Install the reference electrode as shown in the illustrated steps that follow.

At illustrated step 6, carefully turn the collar to break the seal. Then, move the collar up and down

and turn it clockwise and counter-clockwise.

At illustrated step 7, push the collar down and turn the collar less than 1/4 of a turn to lock the collar.

When the collar is locked, the collar does not turn. If the collar is not locked, the KCl electrolyte will

flow too fast from the reference electrode into the measurement cell.

At illustrated step 12, make sure to connect the cable with the blue connector to the reference

electrode.

Keep the storage bottle and caps for future use. Rinse the storage bottle with deionized water.

12 English

Install the sodium electrode

Install the sodium electrode as shown in the illustrated steps that follow.

At illustrated step 3, hold the top of the electrode and point the glass bulb up. Then, quickly invert the

electrode to push liquid down into the glass bulb until there is no air in the glass bulb.

At illustrated step 7, make sure to connect the cable with the black connector to the sodium

electrode.

Keep the storage bottle and caps for future use. Rinse the storage bottle with deionized water.

Examine the electrodes

Make sure that the reference and sodium electrodes do not touch the bottom of the measurement

cell. Refer to Figure 4.

Figure 4 Examine the electrodes

English 13

Fill the KCl electrolyte reservoir

W A R N I N G

Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective

equipment appropriate to the chemicals that are handled. Read the safety data sheet from the supplier

before bottles are filled or reagents are prepared. For laboratory use only. Make the hazard information

known in accordance with the local regulations of the user.

C A U T I O N

Chemical exposure hazard. Dispose of chemicals and wastes in accordance with local, regional and

national regulations.

Note: To prepare 3M KCl electrolyte, refer to Prepare KCl electrolyte on page 36.

Fill the KCl electrolyte reservoir with 3M KCl electrolyte as follows:

1. Put on the personal protective equipment identified in the safety data sheet (MSDS/SDS).

2. Turn the latch on the analytics panel to the unlocked position. Open the analytics panel.

3. Remove the lid from the KCl electrolyte reservoir. Refer to Figure 5.

4. Fill the reservoir (approximately 200 mL).

5. Install the lid.

6. From the front of the analytics panel, squeeze the KCl electrolyte tube with thumb and finger to

push the air bubbles up the tube to the reservoir. Refer to Figure 5.

When an air bubble is near the reservoir, use two hands to squeeze the tube on both sides of the

analytics panel to push the air bubble up.

7. Continue to squeeze the tube until the KCl electrolyte in the reference electrode is at the top of

the glass junction where the KCl electrolyte enters the electrode. Refer to Figure 5.

8. Close the analytics panel. Turn the latch on the analytics panel to the locked position.

Figure 5 Fill the KCl electrolyte reservoir

14 English

Install the stir bar

Put the supplied stir bar in the overflow vessel. Refer to Figure 6.

Figure 6 Install the stir bar

Electrical installation

D A N G E R

Electrocution hazard. Always remove power to the instrument before making electrical connections.

Remove the electrical access cover

Refer to the illustrated steps that follow.

English

15

Connect a power cord—Analyzer with enclosure

The analyzer is available with or without an enclosure. If the analyzer does not have an enclosure, go

to Connect a power cord—Analyzer without enclosure on page 19.

Note: Do not use conduit to supply power.

Item supplied by user: Power cord

5

1. Remove the electrical access cover. Refer to Remove the electrical access cover on page 15.

2. Connect a power cord. Refer to the illustrated steps that follow.

3. Install the electrical access cover.

4. Do not connect the power cord to an electrical outlet.

5

Refer to Power cord guidelines on page 21.

16 English

English 17

Table 6 AC wiring information

Terminal Description Color—North America Color—EU

1 Protective Earth (PE) Ground Green Green with yellow stripe

2 Neutral (N) White Blue

3 Hot (L1) Black Brown

Note: As an alternative, connect the ground (green) wire to the chassis ground. Refer to Figure 7.

Figure 7 Alternative ground (green) wire connection

18 English

Connect a power cord—Analyzer without enclosure

Note: Do not use conduit to supply power.

Item supplied by user: Power cord

6

1. Remove the electrical access cover. Refer to Remove the electrical access cover on page 15.

2. Connect a power cord. Refer to the illustrated steps that follow.

3. Install the electrical access cover.

4. Do not connect the power cord to an electrical outlet.

6

Refer to Power cord guidelines on page 21.

English 19

Table 7 AC wiring information

Terminal Description Color—North America Color—EU

1 Protective Earth (PE) Ground Green Green with yellow stripe

2 Neutral (N) White Blue

3 Hot (L1) Black Brown

Note: As an alternative, connect the ground (green) wire to the chassis ground. Refer to Figure 7 on page 18.

20

English

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