Mettler Toledo QLX3 Liquid Module ユーザーマニュアル

English

Reference Manual QLX3 Liquid Module for XPR Analytical Balances

Deutsch

Referenzhandbuch QLX3-Flüssigdosiermodul für XPR-Analysenwaa-

gen

Español

Manual de referencia Módulo de líquido QLX3 para balanzas analíti-

cas XPR

Français

Manuel de référence Module pour liquides QLX3 pour balances

d'analyse XPR

简体中文

參考手冊 QLX3液体模块适用于XPR分析天平

日本語

リファレンスマニュアル QLX3液体モジュール XPR分析天びん

用

30491778A2021/03/19 6:52- Schema ST4 PDF engine -Layout by Victor Mahler

Reference Manual QLX3 Liquid Module

English

Referenzhandbuch QLX3-Flüssigdosiermodul

Deutsch

Manual de referencia Módulo de líquido QLX3

Español

Manuel de référence Module pour liquides QLX3

Français

參考手冊 QLX3液体模块

简体中文

リファレンスマニュアル QLX3液体モジュール

日本語

Table of Contents

1 Introduction 3

1.1 Further documents and information................................................................................ 3

1.2 Explanation of conventions and symbols used................................................................ 3

1.3 Acronyms and Abbreviations......................................................................................... 4

1.4 Compliance information................................................................................................ 4

2 Safety Information 6

2.1 Definitions of signal words and warning symbols............................................................ 6

2.2 Product-specific safety notes......................................................................................... 6

3 Design and Function 10

3.1 Function description..................................................................................................... 10

3.2 Overview..................................................................................................................... 10

3.3 Components description ............................................................................................... 10

3.4 Dosing head RFID tag .................................................................................................. 12

4 Installation and Putting into Operation 13

4.1 Scope of delivery ......................................................................................................... 13

4.2 Selecting the location ................................................................................................... 13

4.3 Setting up the liquid dosing system................................................................................ 14

4.3.1 Interface of the pump..................................................................................... 14

4.3.2 Wiring the pump........................................................................................... 14

4.3.3 Connecting the tubes ..................................................................................... 14

5 Operation 19

5.1 Liquid dosing .............................................................................................................. 19

5.1.1 Installing and removing the liquid dosing head................................................. 19

5.1.2 Adjusting the dosing height ............................................................................ 19

5.1.3 Attaching the dosing head to the bottle cap ...................................................... 20

5.1.4 Handling the bottle ........................................................................................ 20

5.1.5 Using the QL3 pump ..................................................................................... 21

5.2 Using other weighing methods ...................................................................................... 22

6 Maintenance 23

6.1 Cleaning..................................................................................................................... 23

6.1.1 Cleaning the housing..................................................................................... 23

6.1.2 Cleaning the weighing chamber...................................................................... 23

6.1.3 Cleaning the liquid dosing elements ................................................................ 23

6.2 Replacing the sealing ring and fastening nut on the liquid tube ......................................... 24

7 Troubleshooting 26

7.1 Error symptoms........................................................................................................... 26

8 Technical Data 28

8.1 General data ............................................................................................................... 28

8.2 Model-specific data...................................................................................................... 28

8.3 Material specifications.................................................................................................. 29

8.3.1 Glossary of material acronyms ....................................................................... 29

8.3.2 Liquid dosing head QL001............................................................................. 30

8.3.3 Liquid dosing head QL003............................................................................. 31

8.3.4 QLL standard/advanced kit for bottles .............................................................. 31

8.4 Dimensions................................................................................................................. 32

Table of Contents 1QLX3 Liquid Module

en

9 Disposal 33

10 Accessories and Spare Parts 34

10.1 Accessories................................................................................................................. 34

10.2 Spare parts ................................................................................................................. 38

10.2.1 QLX3 liquid module....................................................................................... 38

10.2.2 QL3 pump.................................................................................................... 38

10.2.3 QLL spare parts kit for bottles ......................................................................... 39

Index 41

Table of Contents2 QLX3 Liquid Module

Introduction 3QLX3 Liquid Module

1 Introduction

Thank you for choosing a METTLER TOLEDO instrument. The instrument combines high performance with ease

of use.

1.1 Further documents and information

u www.mt.com/XPR-automatic

This document is available in other languages online.

u www.mt.com/QLX3-RM

Instructions for cleaning a balance: "8 Steps to a Clean Balance"

u www.mt.com/lab-cleaning-guide

Search for software downloads u www.mt.com/labweighing-software-download

Search for documents u www.mt.com/library

For further questions, please contact your authorized METTLER TOLEDO dealer or service representative.

u www.mt.com/contact

1.2 Explanation of conventions and symbols used

Conventions and symbols

Key and/or button designations and display texts are shown in graphic or bold text, e.g., , Edit.

Note

For useful information about the product.

Refers to an external document.

Elements of instructions

In this manual, step-by-step instructions are presented as follows. The action steps are numbered and can

contain prerequisites, intermediate results and results, as shown in the example. Sequences with less than two

steps are not numbered.

Prerequisites that must be fulfilled before the individual steps can be executed.

1 Step 1

Intermediate result

2 Step 2

Result

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Introduction4 QLX3 Liquid Module

1.3 Acronyms and Abbreviations

Original term Explanation

EMC Electromagnetic Compatibility

FCC Federal Communications Commission

LPS Limited Power Source

POM Polyoxymethylene

RFID Radio-frequency identification

RM Reference Manual

sd Standard deviation

SELV Safety Extra Low Voltage

SOP Standard Operating Procedure

UM User Manual

USB Universal Serial Bus

1.4 Compliance information

National approval documents, e.g., the FCC Supplier Declaration of Conformity, are available online and/or

included in the packaging.

u http://www.mt.com/ComplianceSearch

Contact METTLER TOLEDO for questions about the country-specific compliance of your instrument.

u www.mt.com/contact

United States of America

This equipment has been tested and found to comply with the limits for a Class A digital device, pursuant to

part 15 of the FCC Rules. These limits are designed to provide reasonable protection against harmful inter-

ference when the equipment is operated in a commercial environment. This equipment generates, uses, and

can radiate radio frequency energy and, if not installed and used in accordance with the instruction manual,

may cause harmful interference to radio communications. Operation of this equipment in a residential area is

likely to cause harmful interference in which case the user will be required to correct the interference at his own

expense.

This device complies with Part 15 of the FCC Rules. Operation is subject to the following two conditions:

1. This device may not cause harmful interference.

2. This device must accept any interference received, including interference that may cause undesired

operation.

Changes or modifications not expressly approved by the party responsible for compliance could void the user's

authority to operate the equipment.

Canada

This device contains licence-exempt transmitter(s)/receiver(s) that comply with Innovation, Science and

Economic Development Canada’s licence-exempt RSS(s). Operation is subject to the following two conditions:

1. This device may not cause interference.

2. This device must accept any interference, including interference that may cause undesired operation of the

device.

Singapore

Complies with

IMDA Standards

DA108390

Introduction 5QLX3 Liquid Module

South Africa

TA 2019-1566

APPROVED

Thailand

en

Safety Information6 QLX3 Liquid Module

2 Safety Information

Two documents named "User Manual" and "Reference Manual" are available for this instrument.

The User Manual is printed and delivered with the instrument.

The electronic Reference Manual contains a full description of the instrument and its use.

Keep both documents for future reference.

Include both documents if you transfer the instrument to other parties.

Only use the instrument according to the User Manual and the Reference Manual. If you do not use the

instrument according to these documents or if the instrument is modified, the safety of the instrument may be

impaired and Mettler-Toledo GmbH assumes no liability.

2.1 Definitions of signal words and warning symbols

Safety notes contain important information on safety issues. Ignoring the safety notes may lead to personal

injury, damage to the instrument, malfunctions and false results. Safety notes are marked with the following

signal words and warning symbols:

Signal words

DANGER

A hazardous situation with high risk, resulting in death or severe injury if not avoided.

WARNING

A hazardous situation with medium risk, possibly resulting in death or severe injury if

not avoided.

CAUTION

A hazardous situation with low risk, resulting in minor or moderate injury if not avoided.

NOTICE

A hazardous situation with low risk, resulting in damage to the instrument, other

material damage, malfunctions and erroneous results, or loss of data.

Warning symbols

General hazard Notice

2.2 Product-specific safety notes

Intended use

This dosing system is designed to be used in analytical laboratories by trained staff. The dosing system is

intended for weighing and dosing powder or liquid samples.

Any other type of use and operation beyond the limits of use stated by Mettler-Toledo GmbH without consent

from Mettler-Toledo GmbH is considered as not intended.

Responsibilities of the instrument owner

The instrument owner is the person holding the legal title to the instrument and who uses the instrument or

authorizes any person to use it, or the person who is deemed by law to be the operator of the instrument. The

instrument owner is responsible for the safety of all users of the instrument and third parties.

Mettler-Toledo GmbH assumes that the instrument owner trains users to safely use the instrument in their

workplace and deal with potential hazards. Mettler-Toledo GmbH assumes that the instrument owner provides

the necessary protective gear.

Protective equipment

Chemical-resistant gloves Goggles

Safety Information 7QLX3 Liquid Module

Lab coat

Safety notes

WARNING

Death or serious injury due to electric shock

Contact with parts that carry a live current can lead to death or injury.

1 Only use the METTLER TOLEDO power cable and AC/DC adapter designed for your

instrument.

2 Connect the power cable to a grounded power outlet.

3 Keep all electrical cables and connections away from liquids and moisture.

4 Check the cables and the power plug for damage and replace them if damaged.

WARNING

Injury and/or damage due to hazardous substances

Chemical, biological or radioactive hazards can be associated with the substances

processed by the instrument. During dosing procedures, small amounts of the dosed

substance may become airborne and penetrate the instrument or contaminate its

surroundings.

The substance characteristics and related hazards is the full responsibility of the instrument

owner.

1 Be aware of possible hazards associated with the substance and take adequate safety

measures, e.g., those stated on the safety data sheet provided by the manufacturer.

2 Make sure that every instrument part in contact with the substance will not get altered or

damaged by the substance.

WARNING

Injury or damage due to powder handling

Powders may get compacted in the dosing head and block it. Too much force applied by

the dosing head mechanism may lead to a break and potentially hazardous substances

may get airborne.

1 Handle the dosing heads with care.

2 If the dosing head seems blocked, avoid further dosing. Remove the head from the

instrument and turn it upside down to loosen the powder.

3 Cease work immediately in the event of leak or break.

WARNING

Injury and/or damage due to reacting, flammable, or explosive substances

During the dosing procedure, substances could be combined and cause an exothermic

reaction or explosion. This includes powders, liquids, and gases.

The sample characteristics and related hazards is the full responsibility of the instrument

owner.

1 Be aware of possible hazards associated with reacting, flammable, or explosive

substances.

2 Ensure a working temperature low enough to prevent the formation of flames or an

explosion.

en

Safety Information8 QLX3 Liquid Module

WARNING

Injury or death due to toxic, explosive, or flammable substances

If you use toxic, explosive, or flammable liquids with the pump, the exhaust air will be

contaminated.

Connect a tube to the exhaust air outlet to collect the contaminated air.

WARNING

Injury and/or damage due to reacting substances

When pressure is released from the bottle, the air/gas in the bottle moves back towards the

pump. The air/gas coming from the coupled outlets mixes in the pump. Molecules of the

substances in the various bottles can get in contact through this contaminated air/gas.

1 Do not connect bottles with incompatible liquids to the same pump simultaneously.

2 Before connecting a second, incompatible liquid to the pump, disconnect the first bottle

and purge the pump cavity with clean air/gas.

WARNING

Injury and damage to the pump or the bottle due to high pressure

High pressure from external gas can damage the pump or the bottle.

1 Use a regulator on the external gas line.

2 Ensure that the pressure of the external gas does not exceed 0.5bar (7.2psi).

CAUTION

Injury due to splashing liquids

If the pressure in the bottle is not released, liquid might splash when removing the micro

dosing valve, opening the bottle, or removing the liquid tube.

Always release pressure before removing the micro dosing valve, opening the bottle, or

removing the liquid tube.

CAUTION

Injury due to leaking liquids

Wrongly cut tubing can result in leaking connections.

Cut the tubes with a tube cutter or a sharp knife.

CAUTION

Injury due to moving parts

Do not reach into the working area while parts of the instrument are moving.

CAUTION

Injury due to sharp objects or broken glass

Instrument components, e.g., glass, can break and lead to injuries.

Always proceed with focus and care.

Safety Information 9QLX3 Liquid Module

NOTICE

Damage to the instrument or malfunction due to the use of unsuitable parts

Only use parts from METTLER TOLEDO that are intended to be used with your

instrument.

NOTICE

Damage to the instrument

The instrument contains no user-serviceable parts.

1 Do not open the instrument.

2 In the event of problems, please contact a METTLER TOLEDO representative.

NOTICE

Damage to the instrument due to inappropriate cleaning methods

If liquid enters the housing, it can damage the instrument. The surface of the instrument can

be damaged by certain cleaning agents, solvents, or abrasives.

1 Do not spray or pour liquid on the instrument.

2 Only use the cleaning agents specified in the Reference Manual (RM) of the instrument

or the guide "8 Steps to a Clean Balance".

3 Only use a lightly moistened, lint-free cloth or a tissue to clean the instrument.

4 Wipe off any spills immediately.

en

Design and Function10 QLX3 Liquid Module

3 Design and Function

3.1 Function description

The QLX3 liquid module can be added to XPR analytical balances to perform automatic dosing of liquids. The

liquid dosing head is attached to the liquid module and located inside the weighing chamber. The vertical

position of the liquid module is adjusted manually. The QL3 pump and QLL kit for bottle are completing the

system. The QL3 pump is used to build pressure in the bottle. As soon as the pressure is sufficiently high, the

micro dispensing valve in the liquid dosing head opens and liquid ascends the liquid tube. Several pumps can

be connected to the balance simultaneously and each pump can accommodate up to three bottles (QLL kits).

3.2 Overview

1

2

3

4

5

6

1

Top door

4

ErgoClip vial

2

Liquid module

5

QLL kit for bottle (available separately)

3

Dosing head holder

6

QL3 pump (available separately

3.3 Components description

Dosing head holder

The dosing head holder is where the liquid dosing head is

secured. The dosing head can be released by pressing one

of the release buttons on either side of the holder.

Design and Function 11QLX3 Liquid Module

ErgoClip vial

The ErgoClip vial is used together with vial adapters to

position vials optimally. Those adapters are available for

vials of various diameters and heights. See [Accessories

Page34].

Liquid module

The liquid module is where the liquid dosing head is

attached. It can be moved up and down manually to

adjust the distance between the sample vessel and the tip

of the dosing head.

Top door liquid module

The liquid module is provided with a top door designed

with a slit through which the liquid tube can pass to reach

the inside of the weighing chamber. This door is installed

in the same railings as the standard top door of the

balance and can be opened and closed manually as well

as automatically.

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Design and Function12 QLX3 Liquid Module

3.4 Dosing head RFID tag

1

Each powder and liquid dosing head is equipped with an

integrated RFID tag (1) that stores and exchanges data

with the instrument.

Various data is stored in the RFID tag of the dosing heads,

such as the substance name, lot ID, filling date, expiry

date, etc. It also includes customized data fields.

This data can be edited on the terminal and should be set

before using a new dosing head such that the data is

available for reports and labels.

Installation and Putting into Operation 13QLX3 Liquid Module

4 Installation and Putting into Operation

This instrument must be installed by a METTLER TOLEDO service technician.

The QLX3 liquid module is compatible with all XPR analytical balances with tall draft shield.

4.1 Scope of delivery

QLX3 liquid module

Top door liquid module

ErgoClip vial

Various vial adapters, 4 pcs

Declaration of Conformity

User Manual

The scopes of delivery for the QL3 pump and the QLL kits for bottles are in the documentation delivered with

these products.

4.2 Selecting the location

A balance is a sensitive precision instrument. The location where it is placed will have a profound effect on the

accuracy of the weighing results.

Requirements of the location

Place indoors on stable

table

Ensure sufficient spacing Level the instrument Provide adequate lighting

Avoid direct sunlight Avoid vibrations Avoid strong drafts Avoid temperature fluctu-

ations

Sufficient spacing for balances: > 15 cm all around the instrument

Take into account the environmental conditions. See "Technical Data".

en

Installation and Putting into Operation14 QLX3 Liquid Module

4.3 Setting up the liquid dosing system

4.3.1 Interface of the pump

Rear

Front

11

22

3

4

5

6

1

Air outlets (to bottle)

4

Socket for AC/DC adapter

2

Pressure release button and indicator light

5

USB-B port (to host)

3

Air exhaust outlet

6

Air inlet

4.3.2 Wiring the pump

1 Install the cables in such a way that they cannot be damaged or interfere with operation.

2 Insert the plug of the AC/DC adapter in the power inlet of the pump.

3 Secure the plug by firmly tightening the knurled nut.

4 Insert the plug of the power cable into a grounded power outlet that is easily accessible.

5 Using the USB cable, connect the USB-B port of the pump to one of the USB-A ports of the balance.

4.3.3 Connecting the tubes

Tubes definition

1

2

The liquid tube is the thinner tube (1) used for transporting

liquid from the bottle to the liquid dosing head. The air

tube is the slightly bigger tube (2) used for pumping air

into the bottle. By adding air through the air tube, pressure

rises in the bottle. When the pressure reaches the target

pressure, between 0.3 and 0.5bar (4.4 to 7.2psi), the

micro dispensing valve in the dosing head opens and

liquid can ascend the liquid tube.

1Liquid tube

2Air tube

Preparing the liquid tube

CAUTION

Injury due to leaking liquids

Wrongly cut tubing can result in leaking connections.

Cut the tubes with a tube cutter or a sharp knife.

Installation and Putting into Operation 15QLX3 Liquid Module

The liquid dosing head is inserted in the liquid dosing

head support of the bottle.

1 Using a tube cutter or a sharp knife, cut a sufficient

amount of tubing. The appropriate length mainly

depends on the distance between the balance and the

bottle while dosing.

Recommended length: about 0.9m

0.9 m

D

1 2 2 3

2 NOTICE: Leaking liquid due to wrong assembly. Pay

attention to the orientation of the sealing ring when

threading it on the tube.

Place the sealing ring (1) on a flat stable surface, e.g.,

a table or a workbench, with the wider end

downwards.

3 Take the end of the liquid tube and press it into the

sealing ring.

This is the dosing-head end of the tube. The

opposite end is the bottle end.

4 Thread the two fastening nuts (2), paying attention to the orientation.

5 NOTICE: Leaking liquid due to wrong assembly. Pay attention to the orientation of the sealing ring

when threading it on the tube.

Thread the sealing ring (3) from the bottle end of the tube.

6 Slide the sealing ring until the distance (D) is enough for the tube to reach the bottom of the bottle. Recom-

mended distances for typical bottle volumes are listed next.

Typical distances (D) between the sealing ring and the bottle-end of the tube

Thread Bottle volume Distance (D)

GL45 1000ml 220mm

500ml 170mm

250ml 135mm

GL25 25ml 90mm

Connecting the liquid tube

4

1

2

3

5

1 Insert the dosing-head end of the tube (1) in the

dosing head (2).

2 Tightly fasten the fastening nut to the dosing head.

3 Insert the bottle end of the tube through the corre-

sponding hole in the bottle cap (3). The tube should

reach the bottom of the bottle.

4 If needed, attach the suction filter (4) to the bottle end

of the tube.

5 Tightly fasten the fastening nut to the bottle cap.

6 Screw the cap to the bottle (5).

The suction filter is used to ensure that no particles or

impurities are carried through the liquid dosing head.

Using the suction filter will extend the lifetime of the dosing

head. However, when dosing solutions, molecules of one

of the substances might be absorbed by the suction filter,

altering the concentration of the solution. The suction filter

should only be used when dosing pure solvents.

en

Installation and Putting into Operation16 QLX3 Liquid Module

Connecting the air tube

WARNING

Injury and/or damage due to reacting substances

When pressure is released from the bottle, the air/gas in the bottle moves back towards the

pump. The air/gas coming from the coupled outlets mixes in the pump. Molecules of the

substances in the various bottles can get in contact through this contaminated air/gas.

1 Do not connect bottles with incompatible liquids to the same pump simultaneously.

2 Before connecting a second, incompatible liquid to the pump, disconnect the first bottle

and purge the pump cavity with clean air/gas.

1

2

1 Using a tube cutter or a sharp knife, cut a sufficient

amount of tubing. The appropriate length mainly

depends on the distance between the bottle and the

pump while dosing.

Recommended length: about 0.7m

2 Connect the air tube (1) to the air inlet of the bottle (2)

1

3

4

3 Insert the other end of the air tube (1) in a tube adapter

(3) and press firmly.

4 Connect the tube adapter (3) to one of the air outlets

(4) of the pump. Press until you hear a click.

When a tube is connected to the air outlet of the pump, the

valve of the air outlet opens. Never leave a tube that is

connected to the air outlet unconnected at the other end

because pressure cannot build up.

You can connect up to three bottles to each pump.

Connecting the muffler

1

2

Insert the muffler (1) into the air inlet (2) to absorb the

noise.

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