Lovibond 00386480 - MD1x0/200 - Chloride L (B), Aluminium PP, Copper T, DEHA PP, Hydrazine P, Iron LR L (A), Oxygen dissolved C, Phosphate HR L, Polyacrylate L, Silicate HR PP ユーザーマニュアル

Lovibond® Water Testing

Tintometer® Group

Manual of Methods

MD 100 • MD 110 • MD 200

Oxygen | Phosphate | Polyacrylate | Silica

EN

Manual of Methods

Page 4

DE

Methodenhandbuch

Seite 60

ES

Manual de Métodos

Página 116

FR

Méthodes Manuel

Page 172

IT

Manuale dei Metodi

Pagina 228

PT

Métodos Manual

Página 284

NL

Handboek Methoden

Zijde 340

ZH

方法手册

Page 396

NL Handboek van Methoden 01/20EN Handbook of Methods 01/20

KS4.3 T

0.1 - 4 mmol/l KS4.3

Acid / Indicator

20

S:4.3

Instrument specific information

The test can be performed on the following devices. In addition, the required cuvette

and the absorption range of the photometer are indicated.

Instrument Type Cuvette λMeasuring Range

MD 200, MD 600, MD 610,

MD 640, MultiDirect, PM 620,

PM 630

ø 24 mm 610 nm 0.1 - 4 mmol/l KS4.3

SpectroDirect, XD 7000,

XD 7500

ø 24 mm 615 nm 0.1 - 4 mmol/l KS4.3

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

Alka-M-Photometer Tablet / 100 513210BT

Alka-M-Photometer Tablet / 250 513211BT

Application List

• Waste Water Treatment

• Drinking Water Treatment

• Raw Water Treatment

Notes

1. The terms Alkalinity-m, m-Value, total alkalinity and Acid demand to KS4.3 are iden-

tical.

2. For accurate results, exactly 10 ml of water sample must be used for the test.

Display in the MD

100 / MD 110 /

MD 200

Bar code for the

detection of the

methods

Method name

Measuring range

Chemical Method

Method number

Language codes

ISO 639-1 Revision status

KS4.3 T / 20

How to use

ENMethod Reference Book4

EN

Implementation of the provision Acid capacity KS4.3 with Tablet

Select the method on the device

For this method, no ZERO measurements are to be carried out with the following de-

vices: XD 7000, XD 7500

10 ml

Fill 24 mm vial with 10 ml

sample.

Close vial(s).

Sample

Place sample vial in the

sample chamber. • Pay

attention to the positioning.

Dissolve tablet(s) by inver-

ting.

Sample

Place sample vial in the

sample chamber. • Pay

attention to the positioning.

Test

Press the TEST (XD:

START) button.

The result in Acid Capacity KS4.3 appears on the display.

Performing test

procedure

KS4.3 T / 20

NL Handboek van Methoden 01/20EN Handbook of Methods 01/20

How to use

ENMethod Reference Book 5

EN

Aluminium PP / M50

ENMethod Reference Book1.06

EN

Aluminium PP M50

0.01 - 0.25 mg/L Al AL

Eriochrom Cyanine R

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

VARIO Aluminium Reagent, Set F20 1 Pieces 535000

Preparation

1. To get accurate results the sample temperature must be between 20 °C and 25 °C.

2. To avoid errors caused by contamination, rinse the vial and the accessories

with Hydrochloric acid (approx. 20%) before the analysis. Then rinse them with

deionised water.

Aluminium PP / M50

ENMethod Reference Book1.0 7

EN

Determination of Aluminium with Vario Powder Pack

Select the method on the device.

Blank

20 mL

Prepare two clean 24 mm

vials. Mark one as a blank.

Put 20 mL sample in

100 mL measuring beaker

Add Vario ALUMINIUM ECR

F20 powder pack.

9

4

5

6

7

8

10

11 12

1

2

3

30 sec

Dissolve the powder by

mixing.

Press the ENTER button. Wait for 30 second(s)

reaction time.

Blank

1

Add Vario HEXAMINE

F20 powder pack.

Dissolve the powder by

mixing.

Place 1 drops Vario

ALUMINIUM ECR Masking

Reagent in the blank.

Aluminium PP / M50

ENMethod Reference Book1.08

EN

24 mm

10 mL

Place 10 mL pre-treated

sample in each vial.

Close vial(s). Press the ENTER button.

9

4

5

6

7

8

10

11 12

1

2

3

5 min

Blank

Zero

Wait for 5 minute(s)

reaction time.

Place blank in the sample

chamber. Pay attention to

the positioning.

Press the ZERO button.

Sample

Test

Remove the vial from the

sample chamber.

Place sample vial in the

sample chamber. Pay

attention to the positioning.

Press the TEST (XD:

START)button.

The result in mg/L Aluminium appears on the display.

Aluminium PP / M50

ENMethod Reference Book1.0 9

EN

Analyses

The following table identifies the output values can be converted into other citation

forms.

Unit Cite form Scale Factor

mg/l Al 1

mg/l Al2O31.8894

Chemical Method

Eriochrom Cyanine R

Appendix

Interferences

Removeable Interferences

• A low test result may be given in the presence of Fluorides and Polyphosphates. The

effect of this is generally insignificant unless the water has fluoride added artificially.

In this case, the following table should be used to determine the actual concentration

of aluminium.

Fluoride Displayed value: Aluminium [mg/L]

[mg/L

F]

0.05 0.10 0.15 0.20 0.25 0.30

0.2 0.05 0.11 0.16 0.21 0.27 0.32

0.4 0.06 0.11 0.17 0.23 0.28 0.34

0.6 0.06 0.12 0.18 0.24 0.30 0.37

0.8 0.06 0.13 0.20 0.26 0.32 0.40

1.0 0.07 0.13 0.21 0.28 0.36 0.45

1.5 0.09 0.20 0.29 0.37 0.48 ---

Bibliography

Richter, F. Fresenius, Zeitschrift f. anal. Chemie (1943) 126: 426

According to

APHA Method 3500-Al B

Chloride L (B) / M92

ENMethod Reference Book1.010

EN

Chloride L (B) M92

0.5 - 20 mg/L Cl-CL-

Mercury Thiocyanate / Iron Nitrate

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

Chloride Reagent Set 1 Pieces 56R018490

Chloride L (B) / M92

ENMethod Reference Book1.0 11

EN

Determination of Chloride with liquid reagent

Select the method on the device.

10 mL

Sample

Fill 24 mm vial with 10 mL

sample.

Close vial(s). Place sample vial in the

sample chamber. Pay

attention to the positioning.

Zero

Press the ZERO button. Remove the vial from the

sample chamber.

20

Hold cuvettes vertically

and add equal drops by

pressing slowly.

Add 20 drops

KS251 (Chloride Reagenz

A).

Close vial(s).

Chloride L (B) / M92

ENMethod Reference Book1.012

EN

20

Invert several times to mix

the contents.

Add 20 drops

KS253 (Chloride Reagenz

B).

Close vial(s).

Sample

Test

Invert several times to mix

the contents.

Place sample vial in the

sample chamber. Pay

attention to the positioning.

Press the TEST (XD:

START)button.

9

4

5

6

7

8

10

11 12

1

2

3

5 min

Wait for 5 minute(s)

reaction time.

Once the reaction period is finished, the measurement takes place automatically.

The result in mg/L Chloride appears on the display.

Chloride L (B) / M92

ENMethod Reference Book1.0 13

EN

Analyses

The following table identifies the output values can be converted into other citation

forms.

Unit Cite form Scale Factor

mg/l Cl-1

mg/l NaCl 1.65

Chemical Method

Mercury Thiocyanate / Iron Nitrate

Appendix

Interferences

Persistant Interferences

1. Reducing substances such as sulfite and thiosulfate, that can reduce iron (III) to

iron (II) or mercury (II) to mercury (I) may interfere. Cyanide, Iodine and Bromide

give a positive intereference.

Derived from

DIN 15682-D31

DIN ISO 15923-1 D49

Copper T / M150

ENMethod Reference Book1.014

EN

Copper T M150

0.05 - 5 mg/L Cua) Cu

Biquinoline

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

Copper No. 1 Tablet / 100 513550BT

Copper No. 1 Tablet / 250 513551BT

Copper No. 2 Tablet / 100 513560BT

Copper No. 2 Tablet / 250 513561BT

Set Copper No. 1/No. 2 100 Pc.#100 each 517691BT

Set Copper No. 1/No. 2 250 Pc.#250 each 517692BT

Preparation

1. Strong alkaline or acidic water samples must be adjusted to pH 4 to 6 before

analysis.

Copper T / M150

ENMethod Reference Book1.0 15

EN

Determination of Copper, free with tablet

Select the method on the device.

In addition, choose the test: free

10 mL

Sample

Fill 24 mm vial with 10 mL

sample.

Close vial(s). Place sample vial in the

sample chamber. Pay

attention to the positioning.

Zero

Press the ZERO button. Remove the vial from the

sample chamber.

24 mm

Add COPPER No. 1 tablet

.

Crush tablet(s) by rotating

slightly.

Close vial(s).

Copper T / M150

ENMethod Reference Book1.016

EN

Sample

Test

Dissolve tablet(s) by

inverting.

Place sample vial in the

sample chamber. Pay

attention to the positioning.

Press the TEST (XD:

START)button.

9

4

5

6

7

8

10

11 12

1

2

3

2 min

Wait for 2 minute(s)

reaction time.

Once the reaction period is finished, the measurement takes place automatically.

The result in mg/L free Copper appears on the display.

Determination of Copper, total with tablet

Select the method on the device.

In addition, choose the test: total

10 mL

Sample

Fill 24 mm vial with 10 mL

sample.

Close vial(s). Place sample vial in the

sample chamber. Pay

attention to the positioning.

Copper T / M150

ENMethod Reference Book1.0 17

EN

Zero

Press the ZERO button. Remove the vial from the

sample chamber.

24 mm

Add COPPER No. 1 tablet

.

Crush tablet(s) by rotating

slightly and dissolve.

Add COPPER No. 2 tablet .

24 mm

Crush tablet(s) by rotating

slightly.

Close vial(s). Dissolve tablet(s) by

inverting.

Copper T / M150

ENMethod Reference Book1.018

EN

Sample

Test

9

4

5

6

7

8

10

11 12

1

2

3

2 min

Place sample vial in the

sample chamber. Pay

attention to the positioning.

Press the TEST (XD:

START)button.

Wait for 2 minute(s)

reaction time.

Once the reaction period is finished, the measurement takes place automatically.

The result in mg/L total Copper appears on the display.

Copper T / M150

ENMethod Reference Book1.0 19

EN

Chemical Method

Biquinoline

Appendix

Interferences

Persistant Interferences

1. Cyanide CN- and Silver Ag+ interfere with the test result.

Method Validation

Limit of Detection 0.05 mg/L

Limit of Quantification 0.15 mg/L

End of Measuring Range 5 mg/L

Sensitivity 3.8 mg/L / Abs

Confidence Intervall 0.026 mg/L

Standard Deviation 0.011 mg/L

Variation Coefficient 0.42 %

Bibliography

Photometrische Analyse, Lange/Vedjelek, Verlag Chemie 1980

a) determination of free, combined and total | # including stirring rod, 10 cm

DEHA PP / M167

ENMethod Reference Book1.020

EN

DEHA PP M167

0.02 - 0.5 mg/L DEHA DEHA

PPST

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

VARIO DEHA Reagent Set 1 Pieces 536000

Preparation

1. To avoid errors caused by iron deposits, rinse the glassware with Hydrochloric acid

(approx. 20%) before the analysis and then rinse with deionised water.

Remarks

1. Because the reaction depends on temperature, the temperature must be maintained

at 20 °C ± 2 °C.

2. Keep the sample vial in the dark or in the sample chamber during colour

development time. If the Reagent solution is exposed to UV-light (sunlight) it causes

high measurement results.

DEHA PP / M167

ENMethod Reference Book1.0 21

EN

Determination of DEHA (N,N-Diethylhydroxylamine) with Vario

Powder Pack and Fluid Reagent

Select the method on the device.

Blank

10 mL

Sample

10 mL

Prepare two clean 24 mm

vials. Mark one as a blank.

Put 10 mL deionised

water in the blank.

Put 10 mL sample in the

sample vial.

SampleBlank

Add a Vario OXYSCAV

1 Rgt powder pack in

each vial.

Close vial(s). Invert several times to mix

the contents.

SampleBlank

0.2 mL

Add 0.2 mL Vario DEHA

2 Rgt solution to each

vial.

Close vial(s). Invert several times to mix

the contents.

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Lovibond 00386480 - MD1x0/200 - Chloride L (B), Aluminium PP, Copper T, DEHA PP, Hydrazine P, Iron LR L (A), Oxygen dissolved C, Phosphate HR L, Polyacrylate L, Silicate HR PP ユーザーマニュアル

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